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ҽҩȫ > ҩ > ҩ > Y > ޽

޽

2017-07-24 14:00 Ķ:

йҩ䡷޽

ҩơ޽

ƴYín Yán Huò

ӢHERBA EPIMEDII

֦ҶݡƢţǻ硢Ƿ硢

ԴƷΪС޿ֲ޽Epimedium brevicornum Maxim.Ҷ޽Epimedium sagittatum Sieb.et Zucc.Maxim. ë޽Epimedium pubescens Maxim.ɽ޽Epimedium wushanense T.S.Ying޽Epimedium koreanum Nakaiĸϲġ^Ҷïʢʱɸȥֹʣɹɻɡ

״޽ϸԲΣԼ20cmɫ򵭻ɫ߹󡣾ҶҶСҶƬԲΣ38cm26cmȶ΢⣬СҶΣСҶСƫΣϴ󣬳ʶ״Ե߻ɫë״ϸݣϱɫ±ɫ79ϡϸëϸͻԣСҶ15cmҶƬʡ޳ζ΢ࡣ

Ҷ޽һҶСҶƬ״Σ412cm,2.55cmȶ⣬СҶƫбʼΡ±豻̷ֶëëҶƬʡ

ë޽Ҷ±漰Ҷܱë״ë

ɽ޽СҶƬΣ923cm,1.84.5cmȶ˽򳤽⣬Եߴ̳ݣСҶƬƫбڱƬСԲΣƬΣ⡣±汻ëͺ

޽СҶϴ󣬳410cm,3.57cmȶ˳⡣ҶƬϱ

ȡƷĩ0.5gҴ10ml½30ӣ˹ҺɣҴ 1mlʹܽ⣬ΪƷҺձɫ׷¼ B飬ȡƷҺ[ⶨ]µĶƷҺ10μlֱͬһȼ׻άΪϼĹ轺ȱϣԴͪ-ᣭˮ10:1:1:1Ϊչչȡɣƣ365nm¼ӡƷɫУƷɫӦλϣͬİɫߵ㣻ȻҺƣ365nm¼ӣͬijȺɫӫߵ㡣

ⶨܻͪ ȡ޽ղⶨ¹ƷҺ0.5ml50mlƿУӼ״̶ȣҡȣΪƷҺȡ޽նƷӼ״Ƴÿ1ml10μgҺΪƷҺֱȡƷҺͶƷҺԼΪհףշֹȷ¼ A270nmⶨնȣ㣬á

ƷҶƬƷ㣬ܻͪ޽գC33H40O15ƣ5.0

޽ ոЧҺɫ׷¼ Dⶨ

ɫϵͳ ʮϹ轺Ϊ-ˮ30:70ΪࣻⲨΪ270nm۰޽շӦ1500

ƷҺƱ ܳȡ޽նƷӼ״Ƴÿ1ml0.1mgҺá

ƷҺƱ ȡƷҶƬĩ40ĿɸԼ0.2g[ͬʱȡƷҶƬĩⶨˮ֣¼ H һ]ܳƶ50ml׶ƿУܼϡҴ20mlƶ1СʱٳƶϡҴʧҡȣ˹ȡҺá

ⶨ ֱȡƷҺ빩ƷҺ10μlעҺɫǣⶨá

ƷҶƬƷ㣬޽գC33H40O15 0.50

ơ޽ȥʣժȡҶƬˮ˿

޽ȡ֬ͼۻ޽˿Ļйȡÿ100kg޽֬ͣͣ20kg

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ΡǿǣʪžʪʹľΣڸѪѹ

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ƴYín Yán Huò

ǰƢ׹ۡݼȲݡȲݡǧ𡢸ɼ棨ջӱݡ֦Ҷݣͼţǻͭ˿ݡƣ䷽ҩǡξݡǣҩ־

ԴΪС޿ֲ޽Ҷ޽Ҷ޽ҶġգȡҶȥʣɹɡ

ԭ̬޽

ݱ3040סߣӲҶΪ23ҶСҶ9ƬгСҶƬʣԲΣ4.59ף3.57.5ףȶ˼⣬Եϸݣȶ˳ɴ״ëΣСҶбΣʱëë䣬гë46״򣬻ëżëԼ1ףаƬ״ΣĤʣֱԼ2ףưɫɫ8Ƭ״Σ2֣4ƬСͬΣ4ƬϴͬΣ4ԲΣ߳ࣻ41uȋĴΣʱ2ѡ45¡56¡

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ϼֲĸ޽๩ҩãר

ϵӦõ޽ԭֲΪҶ޽ҶΪ3СҶҶСҶƬҶë״1015仨СëڲĻ೤һ

ֲɽĴȵء

״޽Ҷ޽

ᆬϸԲΣпգ2030.ɫɫ⣬ëҶ.Ϊһ֦һ֦ҶҶƬ״Σȶ˼⣬ΡԵϸ״ݣɫ⻬ɫϸͻҶֽеԡζࡣ

Ҷ޽СҶ޽ҶƬΪԲΣȶ΢⡣޽ͬ

ۼҶ޽

ҶƬΪ״ΣʣҶ˽ʴ״ҶΡ޽ͬ

ҩľԹ١Ҷࡢɫ̡Ϊѡ

ѧɷ֡޽Ҷ޽߰Ҷкӷ͡ئһ顢ֲ޴ʡ֬֬е֬ᡢӲ֬ᡢᡢᡣ

ҩáٶԻܵӰ

޽дãھҺڿҳ󣬴̼о񾭣˷޽ձ޽Ƴɵ࣬Թ䲻ܱ־βӦ֪дٽҺڵãҶǿʵ֮ǰ١ҡؼķС֤޽ȡҺԼãЧߴǿʼ򻼰עȡҺ2040ˣЧ൱7.5΢غء޽ժѳС֤޴ԼصãԴʡڡСдԼصųӰ죬ˮˮͬձ޽ҴȡȥѳСӰ죬಻ӹѳ

ڶ΢Ӱ

޽ԹڶԼײŵãҩ벡Ӵ1Сʱڣãƣ԰ɫɫ־ãϿ˫Ѫ˾á1Ũȶͽ˸˾־Ч

ȡ̵ƽ

޽ĸƼУԾҶƷȡC޽ţ޽Ҷ=821һ̵ãСӺ취ȡΪãSO2СԷ֧ƽò롣

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ܡҽѧš"飬ƫ㲻죬֫Ƥʡ"

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ۡ"޽ˣջӡӾŮӾνšҲΪ֮֮ԪҲν֮Ԫ֮ڼ¡νǿ־μ֤Ԫ֮ʡʹС㲻Ը£ζԪDzͬһҲ˻룣꽡Ԫ˥ܶҲ˼֪ӡ֪ζԽΪܽҲ"

ܡ塷"޽£ר׳Իߣ֮Ҳʹ֮麮Сߣָ˼麮֮²С֮䲹Сʪ̽ᣬˮɬ߿ɱȣᡣǿ־ǣԪ֮Ȼ麮߹ˣ䣬ߣ򲻿Ϊ֮ҲߡӸͨѪᡣȻ֮Ѫ䣬ƣ尾Һ̵Ϊ࣬飬档ϴ²֮ܳʪȣߴϴɱջɷŮӾһμ֫ʣϥ֮Ʒ̲׳ͨо磬纮ʪԡջν˻룣꽡δ̫֮ν˥Ů˥֮ߣ˷֮ƫ²̶֮࣬ӡʯνһζƢƣΪƫ粻Ҫҩ֮жһΪѪ飬磬纮ʪȱ֮֮ν֢ҲҲһΪѪϳ壬񾭶ʧ˶֮֮νз磬ҽ֮νԾҲ䲡ҲƢƣֹη纮ʪ֮죬Ѫ֮죬ѪԾ֮죬򲻿á"

ٴӦáС֢

ȡ޽ɣƳÿ2ҩ1˵עҺԼעΪѨλע䡣עÿ2ÿ2Σ20졣ָڼ֢ѨλעΪϼע䡣Ѩλע䰴ȡѨÿѨע121Σ20죬ϢټơƸС֢246мڻ34Ȭ8Ȭ16Ч7Ч2Ч1ָڻ43Ȭ21Ч155Ч2֢ڻ߹169ȬȬ9ЧЧ129Ч31ݹ۲죬ƷԼڼսָڵIJЧָϿ졣Ժ֢ҲһЧҩ֫ձзȡоȸоЧɼ𽥻ָ֣֫һ֫ЧϺã֫ԼϴЧϲҩпڸ⣬δá

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ƴYín Yán Huò

ӢHerb of Shorthorned Epimedium, Herb of Sagittate Epimedium, Herb of Pubescent epimedium,Herb of Korean Epimedium,Epimedium Herb

ǰƢ桢ȲݡȲݡ硢硢ڡͷ硢޽ҶǷ硢ݡǧ𡢸ɼצ֦Ҷݡţǻͭ˿ݡơǡξݡǡ

ԡũݾ

1ͼ޽񽭶̩ɽС֮ҶҶд̡ڸѡɫ롣¿ɫɫСͷӡ²ҶɹɡߣҶС֦ϸ񣬸ƻйȺ֦ҶݣһҶ㿰ʹ

2Ŀ޽ɽڣһߣһߣһ⣬һҶҶ磬Ҷ

ԴҩĻԴΪС޿ֲ޽ǰҶ޽Ҷ޽ɽ޽޽ë޽ȵľҶ

ֲﶯ1.Epimedium brevicornum Maxim.2.Epimedium sagittatum.3.Epimedium wushanense.4.Epimedium koreanum Nakai.5.Epimedium pubesens Maxim.

պʹأġգȡҶȥʣɹɡ

ԭ̬1.޽ݱ30-40cmߣֱ3-5mmӲֱ⣬ëͨ޻ҶҶ2ھгҶСҶ9λԲΣ3-7cm2.5-6cmȶ˼̽⣬ΣԵд̳ݣɫйë²԰ɫëԣСҶƬԲΣȣСҶƬԳƣڲԲΣ༱⡣Բ׶10-35cmἰëƬ״ΣĤʣɫֱ1.5,20-50䣬㳤5-20mmƬ4Σɫ1-3mm,Ƭ4Σɫ򵭻ɫԼIcm2-4mm,4С೤2-3mm43-4mmҩԼ2mm;1uȋIcmȶ๡1-2ţɫ5-6£ 6-8¡

2.Ҷ޽ ̲ݱ25-50cm̴֣Գʽ״ӲƤɫɫ⣬ëҶ1-3mmһҶҶϸ4-18cmҶ2ھҶͬͣСҶʣΣ15-19cm3-8cmȶ˼򽥼⣬ΣΣСҶʲԳΣdzѣԵϸëëϸӲëСҶƬԲΣȣСҶƬԳƣڲƬСͼΣƬϴΣ⡣Բ׶ֱͦἰͨëʱëɫֱԼ6mm20-60仨ԼIcmƬ4Բ״Σ3-4mm,1.5-2mmɫƬ4λ״ΣԼ4mmԼ2mmȶ˼⣬ɫƬȳػɫж̾ࣻ4Լ5mmҩѣԼ3mmuȋԼlcm,๡״ԲΣԼ4mmɫ2-3£5-6¡

3.ɽ޽ ̲ݱ50-80cm״Ӳ汻ɫƬܶһҶ߳СҶ3СҶ߱ҶƬʣΣ9-23cm1.8-4.5cmȶ˽򳤽⣬ΣԵʴ̳ݣСҶ߾ȵԲƬСҶƬƫбڲƬСԲΣƬΣ⣬汻ëͺ2öҶԲ׶15—30cmż50cm߶ë豻ëëɫֱ35cmƬ4ԲΣ2-5mm1.5-3mmƬԲΣ3-15mm1.5-8mmȶ˶ۣʽ״࣬ɫʱɫ06-2mmﳤ2—4mmƤбԲ״г10-12顣uȋԼl5cm4-5£6¡

4.޽ ݱ20-40cmߣӲֱ⣬2-3öƬҶͨޣϡ1-2뾥ȳҶΪҶlöھг뾥Ӵ߹ؽڣСҶ9СҶһҶСҶƬΣڳԼ5cmԼ3cm󣬳Լ10cmԼ7cmΣбȶ⣬Եë״΢ϸݣëʱëë䡣״Ҷ̣뾥Ҷھ࣬һɻ磬г߹ؽڣë2öС4—6仨СԼIcmϴֱ2cmƬ8״Σ3-4mmɫ4ƬС4Ƭϴ󣬳6-9mm4ɫưɫԲΣ7-8mmȶ˼⣻ӷ1ң쳤ͷͷ״uȋĴΣԼ6mm2ѣСѰ䣬޴棬6-8ӡ4Ѯ5Ѯ5¡

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2.ֲࡢաա㽭̨塢ϡ㶫Ĵݵȵء

3.ֲĴݵȵء

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״޽ʣȥ˿ɸȥм޽ȡ֬ùڼۻȥټ޽΢֬ͻȡ(ÿ޽100ɵ֬25)

ѧɷ֡1.޽ϲֺ޽ͪ߰icariin޽ͪ߰icarisideIءƵ޻Ԫء

2.Ҷ޽ȫݺ޽ͪ߰ʽζʣʣӷͣʮceryl alcoholʮ飨triacontaneֲ޴phytosterolᣨoleic acidᣨlinoeic acid֬ᣨPalmitic acid)ƤأquercetinƤ-3-O-β-D-߰quercetin-3-O-β-D-glucoside⣬ص޻Ԫأױ޽ͪ߰I޽-3-߰icaritin3O-a-rhamnoside)ˮ޽-3-߰anhydroicaritin-3-O-a-rhamnoside)Ҷ߰sagittatosideABC޽epimedinABcҶͤ߰(sagittatin)ABϲֺ޽߰icarisideA1B2B6B9D3E6E7H1޽߰ԪB1 icarisidinB1޽ icariolA1A2ʽʽ񴼣dilignol)55’񴼣55'dimethoxydilignolʽʽ߰dilignol rhamnosidʽ 5’һ߰5’methoxydilignol rhamnosideʽʽ12һ˫һ4ǻһ3һһһl3һl2-bis-(4-hydroxy-3-methoxyphenyl)-propane-1,3-diol,5һ--Ҷ֬5methoxy--(solaritiresinolҶ֬5һ9һľǻ---Ҷ֬-֬أolivil֬-߰syringaresinol-O-βD-glucopy-glucopy-ranosideɽ֬߰symplocosigenin-O-β-D-glucopyra-nosideȥ˫ɰش dihydrodehydrodiconiferylalcoholҴ߰Phenethyl glucosideZ--3-ϩ߰(z)-3-hexenyl glucoside,¬Ŵ C߰blumenolC gfucoside

3ɽ޽ϲֺ޽ͪ߰ɽ޽ͪ߰wushanicariin޽߰baohuoside IVI޽߰rouhuosideƤ-3-߰Ƥ-3-߰޽߰(epimedosideA޽أ8-ϩɽͷ-4’--3-ľǻ l→4߰ݣ7߰8-prenylkaempferol-4'-methoxy-3-xylosyl(1→4)rhamnoside-7-glucosideкƵ޻Ԫء

4.޽ϲֺ޽ͪ߰޽߰A޽ ABC޽A1B1Ƥأˮ޽-3-߰޽߰epimedokoreanodide)I򣬴ӵ²ֵַöʮ飨n-nonacosaneʮһ飨nhentriacotane޴campesterolβ-޴β-sitosterolβ-޴-3-߰ij޴-3-߰2”-⿨߯ A2”Orhamnosylikarisoside A2”-޽ͪ߰޽ͪ߰߰A⿨߰ ikarisiosideA޽߰baohuoside򣬴кƵ޻Ԫء

5ë޽ϲֺ޽ͪ߰޽ͪ߰I޽߰C޽߰򡢢˿߰hyperosde޽߰кƵ޻Ԫء

⣬ֲͬҶϲֺƵ޻Ԫء޽ϲֺƵ޻Ԫء޽ȫݺ޽ͪ߰޽߰AC޽أȥ޽أ߰񡢢򡢢󡢢޽أbaohuosuСأtricinɽͷ-3-˫߰kaemPfero3-dirhamnoside)˿߰кƵ޻Ԫء

ҩá1.ԹܵӰ죺ƷٽԹھҺڿҳ󣬴̼о񾭣˷Ȯθ޽ˮ࣬䲻βӦɴٽҺķڣҶǿʵ֮Сǰ١ҡؼӷʵ֤޽ȡ20-40mgעЧ7.5μg غ൱׻޽17̴ͪ24СʱйƽֵԻ˵ˮƽ17Ƥ̴24СʱйδԸơʾ޽һĴٽٹܵá

2.ȡ̵ƽãСӺڷ֤ƷƷ͸Ʒȡһ̵áСȷ֤״ȡáǰ߻ȫõ̼èĿԣԵģ״ȡ鰷Ҳбá

3.ԭ΢ãƷ԰ɫɫнŵãϿ˫Ѫ˾ã1%ŨԹڿƽ˸˾޽Լײ没A9B4B5ͼECHO69͵ȾãÿǶԲֱ

4.Ѫϵͳã4.1ѹãƷҴҺã2.5mlkgè2mlkg4mlkgע,ʽѹãԶõΪԡ͸ѪѹθƷ״ȡ10gkgɳԵѪѹ½ͣҩѪѹѪѹ۲쵽޽˫ྱܶļѹ䣬ȥصѹãèע䰢Ʒ󣬱ƷнѹãǿԼƵ̼è񾭽ǰά˲ĤӦԵ̼ںάķӦáΪ޽Ľѹa弰M-ϵͳ޹أҪ뽻񾭽йء

4.2ãĹʵ֤޽Һ200%޽ˮƬȡķǰᲿ֣No5-1-1ĵĹƽȸҩǰ75.3%200%޽0.5mlʹƽ126.6%ȮעNo5-1-1 1gkgӰ죬ӣͬʱŵؼٹþעNo5-1-1󣬱ֳһԵĽѹãжݽѹãýNo5-1-1ԴҶ´ļȱѪбãԶë߰Kزʵɲ룬ȻȫԿʱ䡣ûⶨļȽ֤No5-1-1 Ƽ2mglСʱļ

5.СѹȱӰ죺С ǻע 100%޽0.1-0.15mlСȱһıá

6.Ѫ֬Ӱ죺ʵԸ֬Ѫ֢ θ 100%޽ÿ5ml2Σ,30죬ҩ102030죬B-֬׼̴½ֻڸҩ10½2030

7.ѪǵӰ죺ʵԸѪǴθ޽ȡҺ10mgkgԽѪãɳ60ϡ

8.ãƤע޽״ȡ50mgkgԼᵰԽͳ̶ȣùθ 15gkgܽ֯ëϸѪͨ͸ӡ

9.߹ܵӰ죺޽ܻͪʹСγϸܼζڻָŴٽСܰϸָ̼ʹ֮ӽ޽ܻͪСѪѪؿˮƽƢ࿹ϸٽPHA̼ܰϸתӦǿǻϸɹܡë޽50%״ȡҺǿСܰϸConALPSֳӦСܰϸӦҩŨȳأ飬СθɲӳֲͬĴڡ

10.ѪСۼԺѪҺѧӰ죺޽ǺܻͪɴٽADPյѪСۼǿΪǣܻͪ߱յѪСۼá޽ȴԽADP յĽѪСۼʣɴٽѪСۡ˿ڷ޽󣬺ѪѹԼ٣ϸӾʱ̣Ѫӿ죬ӶʹȫѪճԽ͡

11.ԺлӰ죺ǻСθ޽ˮҺDNAϳʡ޽飬ʹǻСĹϸֳ72%DNAϳ68%

12.ã޽ԶӰ׿ãĵðơСǻע10%޽20mlkgԵáɵMcGMPϵͳƷԻܣӸѪغͪп˥á

ԡձ޽ʹܵͫʹС˶ӣܿȾΣֹͣںֹͣһʱڳ޽СǻעΪ36gkgNo5-1-1СעİΪ56.8±2.7gkgƷ״ȡĶԵͣСθ 450g/kg۲3,޶ԷӦձʹܵͫС˶ӣܿȾΣֹͣ

1.ȡĩ1gҴ20mlȻ1СʱҺŨ5mlȡ1mlԹУþٻҡȣŨΣˮԡ1-2ӣԺɫͪ2.ȡĩ0.5gҴ10ml½30ӣ˹ҺɣҴ1mlܽ⣬ԣȡ޽߰ҴҺաȡҺ1μlڹ轺H-CMC(0.5%)Դ-ͪ--ˮ(10:1:1:1)չ15cmȡɣ(365nm)¼ӣƷһɫߵ㣬1%ȻҴҺ¼ӣԳȺɫ

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ƫ磬㲻죬ƤʣƢһϸﱣʢڲУ޻Ҿƶ֮Ժֽܷ⣬ͨգﶬաÿů֮ô(ʥݷ)ηעʹƢһһܺ˕—һԶһҩϸΪɢÿʱ¾ƵһǮ(ʥݷƢɢ)Ŀ裺Ƣ(С¥ɫ)ȷ֡ΪĩÿһǮ£ն(ʥ¼)ۣƢж٣Ϊĩݡ(Чɢ)

1.Ŀ޽²澫֮

2.ݾ衷޽¶޶ԺߣҲǿ־ʹߣҲʹֹӡߣݶ֮٣Һɣܳӣ仯СҲǣԼӡɢᣬܻУͨѪ߳Ӹ²дϴ档

3.޽ˣջӡӾŮӾνšҲΪ֮֮ԪҲ ν֮Ԫ֮ڼ¡νǿ־μ֤Ԫ֮ʡʹС㲻Ը£ζԪDzͬʿҲ˻룣꽡Ԫ˥ܶҲ˼֪ӡ֪ζԽΪܽҲ

4.塷޽£ר׳Իߣ֮Ҳʹ֮麮Сߣָ˼麮֮²С֮䲹Сʪ̽ᣬˮɬ߿ɱȣᡣǿ־ǣԪ֮Ȼ麮߹ˣ䣬ߣ򲻿Ϊ֮ҲߡӸͨѪᡣȻ֮Ѫ䣬ƣ尾Һ̵Ϊ࣬飬档ϴ²֮ܳʪȣߴϴɱջɷŮӾһμ֫ʣϥ֮Ʒ̲׳ͨо磬ʪԡջν˻룣꽡δ̫֮ν˥Ů˥֮ߣ˷֮ƫ²̶֮࣬ӡʯνһζƢƣΪƫ粻Ҫҩ֮жһΪѪ飬磬纮ʪȱ֮֮ν֢ҲҲһΪѪϳ壬񾭶ʧ˶֮֮νз磬ҽ֮νԾҲ䲡ҲƢƣֹκʪ֮죬Ѫ֮죬ѪԾ֮죬򲻿á

ٴӦá1.С֢ȡ޽ɣƳÿ2mlҩ 1gעҺԼעΪѨλע䡣עÿ2mlÿ2Σ20졣ָڼ֢ѨλעΪϼע䡣Ѩλע䰴ȡѨÿѨע1-2ml1Σ20죬ϢټơƸС֢246мڻ34Ȭ8Ȭ16Ч7Ч2Ч1ָڻ43Ȭ21Ч155Ч2֢ڻ߹169ȬȬ9ЧЧ129Ч31ݹ۲죬ƷԼڼսָڵIJЧţָϿ졣Ժ֢ҲһЧҩ֫ձзȡоȸоЧɼ𽥻ָ֣֫һ֫ЧϺã֫ԼϴЧϲҩпڸ⣬δá

2˥213%޽Һ͸뷨ÿ1Σ10-20ΪһƳ̡򾲼۲104Ȭ22Ž2146Ч15Ƴ̳ЧϺãƺ֢״ʼת磬Чã15β޺תߣʹƣЧ಻ţҲ̡ƳڿɳȷӦ֢״ʱأƼѸʧ

2220%޽ÿ5mlÿ3ηǰ2-3¡50Լ80%κ֢״ᡣҩڼδӦ˷ܹռƻѪѹߡ

3ףԵζ޽۲1000һƳ̵ЧΪ74.6%ڿƺЧΪ22.1%ϰزɸƣЧߡʵ֤͵ЧڴϢͣЧϲ̳ЧԹϵ̵ýϺãƽϲƳ߱һƳ̵ĽڿƺЧߡ۲ԾһƳ̵110ãЧΪ59.1%ԭЧ½26.1%Ƽ÷ȡ޽Ҷ(Ʒ)80%ȡŨ֭20%зۣ߻Ϊ衣ÿ൱ҩ1ηַ൱ҩ5Ǯ1.5ļ(һ)ֱԲֲй۲죬Чշ1߾ơҩ󲿷ֲ΢ӦԿڸɡΪΪ͡ͷΣһʧ

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